📋 Summary
- Comparison Table: Full vs. Reduced Direct Verification
- Calculation Methods — All ISO 148-2 Quantities
- Potential Energy Ep
- No-load Losses (p + p')
- Expanded Uncertainty U (variable k)
- Table 2 — Criteria b and Bv
- Interpretation of the Report
- Measured Balance — Complete Example
- Compliance Conclusion
- Validation in Real Conditions
Calibration Methodology
The calibration of a Charpy impact testing machine is based on two complementary levels of verification defined by ISO 148-2 and ASTM E23: direct verification (measurement of physical quantities) and indirect verification (traceable CRMs from NIST/BAM/IRMM). Uncertainty is evaluated according to GUM (JCGM 100:2008).
⚠️ Note ISO 148-2 §A.1.2: U(KV) is provided for information only. Compliance with Table 2 (b and Bv) is assessed directly without a guard band, unless otherwise instructed by the customer.
1. Comparison Table — Full vs. Reduced Direct Verification (ISO 148-2)
📌 Frequencies (§8): Full = installation, relocation, unsatisfactory indirect results | Reduced = before each indirect verification + daily use (§8.5)
| Verification | Ref. § | Full | Reduced | Criterion / Tolerance |
|---|---|---|---|---|
| 🏗️ FOUNDATION AND FRAME | ||||
| Machine level | §6.2.1 | ✅ | — | Level bubble centered |
| Ground fixing / bolts | §6.2.3a | ✅ | ✅ | Manufacturer's torque |
| Frame rigidity | §6.2.2 | ✅ | — | No visible deformation |
| ⚙️ PENDULUM | ||||
| Hammer mass m | §6.3.1 | ✅ | — | Nominal ±0.1 % |
| Center of percussion L | §6.3.2 | ✅ | — | L = g×T²/(4π²) | ±1 % of L_nominal |
| Impact velocity v | §6.3.3 | ✅ | — | v = √(2gL(1−cosα)) | 5.0–5.5 m/s |
| Axial bearing play | §6.3.8 | ✅ | ✅ | < 0.25 mm |
| Lift angle α | §6.3.4 | ✅ | — | Nominal ±0.3° |
| 🔪 STRIKER AND ANVILS | ||||
| Striker radius | §6.3.5 | ✅ | ✅ visual | 2.5 mm (±0.5) or 8 mm (±0.5) |
| Striker angle | §6.3.5 | ✅ | ✅ if changed | 90° ± 2° |
| Distance between anvils | §6.3.6 | ✅ | — | 40 ±0.2 mm |
| Anvil radius | §6.3.6 | ✅ | — | 1.0 mm (±0.07) or 1.5 mm (±0.07) |
| Specimen centering | §6.3.7 | ✅ | — | ±0.5 mm |
| 📊 ENERGY MEASUREMENTS | ||||
| Potential energy Ep | §6.4.2 | ✅ | — | KN ±1 % | Ep = m×g×L×(1−cosα) |
| Index losses p | §6.4.5.1 | ✅ | ✅ | p = K1 − K2 (4 determinations) |
| Bearing+air losses p' | §6.4.5.2 | ✅ | ✅ | p' = (K3−K2)/10 (10 half-oscillations) |
| Total losses p+p' | §6.4.5.3 | ✅ | ✅ | < 0.5 % of KN |
| KS indicator (6 points) | §6.4.3 | ✅ | ✅ | |KS−Kcalc|/Kcalc <1% (≥50%KN) or <0.5%KN |
| 🧪 INDIRECT VERIFICATION (CRM) | ||||
| Number of CRM levels | §7.2 | ✅ ≥2 | ✅ ≥2 | Min. 2 levels, ≥5 specimens/level |
| Repeatability b = KVmax−KVmin | Table 2 | ✅ | ✅ | ≤6 J (KVR<40J) | ≤15%×KVR (KVR≥40J) |
| Error |Bv| = |KV̄v−KVR| | Table 2 | ✅ | ✅ | ≤4 J (KVR<40J) | ≤10%×KVR (KVR≥40J) |
2. Calculation Methods — All ISO 148-2 Quantities
| Quantity | Normative formula | Reference | Numerical Example |
|---|---|---|---|
| 📐 DIRECT VERIFICATION | |||
| Center of percussion L | L = g×T²/(4π²) | §6.4.6 Eq.13 | T=1.824s → L=0.826 m |
| Potential energy Ep | Ep = m×g×L×(1−cosα) | §6.4.2 Eq.1 | 23.17×9.807×0.826×1.766 = 331.4 J |
| Impact velocity v | v = √(2×g×L×(1−cosα)) | §6.3.3 | √(2×9.807×0.826×1.766) = 5.35 m/s |
| Index losses p | p = K1 − K2 | §6.4.5.1 | Avg. 4 tests with/without index |
| Bearing losses p' | p' = (K3 − K2) / 10 | §6.4.5.2 | 10 half-oscillations |
| Total loss E_vide | E_vide = p + p' | §6.4.5.3 | 1.85+1.78 = 3.63 J = 1.10% KN ❌ |
| KS Indicator | Kcalc = m×g×L×(cosβ−cosα) | §6.4.3 Eq.2 | 6 points: 0,10,20,30,50,80% KN |
| 🧪 INDIRECT VERIFICATION (ISO 148-2 Annex A) | |||
| Bias Bv | Bv = KV̄v − KVR | Eq. A.1 | 111.8 − 108.0 = +3.8 J |
| Repeatability b | b = KVmax − KVmin | Table 2 | 114 − 109 = 5 J ≤ 16.2 J ✅ |
| u(KV̄v) | u(KV̄v) = sv / √nv | Eq. A.2 | 1.924/√5 = 0.860 J | νB=4 |
| u(Bv) | u(Bv) = √[u²(KV̄v)+u²RM] | Eq. A.3 | √[0.860²+2.5²] = 2.645 J |
| uv | uv = √[u²(Bv) + Bv²] | Eq. A.4 | √[2.645²+3.8²] = 4.635 J |
| νv (Welch-Satterthwaite) | νv = uv⁴/[u⁴(KV̄v)/νB + u⁴RM/νRM + Bv⁴/νB] | Eq. A.5 | νRM=∞ → νv calculated |
| 📏 TEST UNCERTAINTY (ISO 148-1 Annex E) | |||
| u(x̄) repeatability | u(x̄) = sx / √n | Eq. E.3 | νx = n−1 |
| u(r) resolution | u(r) = r / √3 | Eq. E.4 | r=0.5J → u(r)=0.289 J |
| u(KV) combined | u(KV) = √[u²(x̄)+u²v+u²(r)] | Eq. E.5 | √[0.860²+4.635²+0.289²] = 4.730 J |
| νKV (Welch-Satterthwaite) | νKV = u⁴(KV)/[u⁴(x̄)/νx + u⁴v/νv] | Eq. E.6 | νKV ≈ 53 |
| k = t95(νKV) | Table E.5 ISO 148-1 | Eq. E.7 | νKV=53 → k=2.01 ≈ 2.0 |
| U(KV) expanded | U(KV) = k × u(KV) | Eq. E.7 | 2.0 × 4.730 = 9.46 J ℹ️ informative |
3. Potential Energy Ep
Ep = m×g×L×(1−cosα) = 23.170×9.8065×0.826×1.766 = 331.4 J ⚠️ Adjust α (nominal 300 J)
📐 Origin of values (ISO 148-2 §6.4.2, Eq.1):
m = 23.170 kg — Hammer mass (±0.1 %)
g = 9.8065 m/s² — Certified local value from IGN
L = 0.826 m — Center of percussion via T=1.824 s: L=g×T²/(4π²)
α = 140° — Lift angle (±0.3°)
⚠️ Ep = 331.4 J exceeds 300 J by +10.5 % → Recalibrate α to 126.8°
m = 23.170 kg — Hammer mass (±0.1 %)
g = 9.8065 m/s² — Certified local value from IGN
L = 0.826 m — Center of percussion via T=1.824 s: L=g×T²/(4π²)
α = 140° — Lift angle (±0.3°)
⚠️ Ep = 331.4 J exceeds 300 J by +10.5 % → Recalibrate α to 126.8°
4. No-Load Losses — Normative Procedure (§6.4.5)
⚠️ E_vide = p + p' — DO NOT subtract from individual KVs. Used only for direct compliance criterion.
Step 1 — Index Friction p (§6.4.5.1)
Test with index → K1 | Without moving index → K2 | p = K1 − K2 | Average of 4 determinations
Step 2 — Bearing + Air Friction p' (§6.4.5.2)
10 half-oscillations → K3 | p' = (K3 − K2) / 10
Step 3 — Criterion (§6.4.5.3)
E_empty = p + p' < 0.5% of KN | For KN=300 J → E_empty < 1.5 J | Example: 1.85+1.78 = 3.63 J = 1.10% → ❌ NC
5. Expanded uncertainty U(KV) — k variable
See Table Section 2 for all formulas. Numerical application: u(KV)=4.730 J | νKV=53 | k=2.01 | U(KV)=9.46 J (informative §A.1.2)
⚠️ k ≠ 2 if νKV < 30. Always calculate νKV via Welch-Satterthwaite before choosing k (Table E.5 ISO 148-1).
| ν | k=t95(ν) | Typical case | ν | k=t95(ν) | Typical case |
|---|---|---|---|---|---|
| 2 | 4.30 | n=3, dominant uv | 10 | 2.23 | n=3, low energy |
| 3 | 3.18 | 15 | 2.13 | ||
| 4 | 2.78 | n=3, high energy | 20 | 2.09 | |
| 5 | 2.57 | n=5, strong uv | 30 | 2.04 | |
| 7 | 2.36 | Ex. standard A.1 (νv=7) | 50 | 2.01 | n=5, νKV≈53 ✅ |
| 8 | 2.31 | Ex. standard E.3 (νKV=8) | ∞ | 1.96 | Normal distribution |
6. Table 2 — ISO 148-2 conformity criteria
| KVR Level | b max (KVmax−KVmin) | |Bv| max | For KVR=108 J |
|---|---|---|---|
| KVR < 40 J | 6 J | 4 J | — |
| KVR ≥ 40 J | 15% × KVR | 10% × KVR | b≤16.2 J | |Bv|≤10.8 J |
✅ Example: b=5 J ≤ 16.2 J ✅ | |Bv|=3.8 J ≤ 10.8 J ✅ — Direct conformity without guard band (§A.1.2)
7. Interpretation of the report (§9 ISO 148-2)
| Section §9 | Mandatory content |
|---|---|
| §9.1 General | Reference ISO 148-2:2008, manufacturer, model, serial no., knife radius, owner, date |
| §9.2 Direct | KN, impact velocity, empty losses p+p' |
| §9.3 Indirect | CRM (KVR, KV_read), b=KVmax−KVmin, Bv, conformity Table 2, informative U(KV) |
8. Measured balance — Complete example (ZR-2019-0047)
| Quantity | Value | Criterion | Status |
|---|---|---|---|
| Center of percussion L | 0.8264 m | 0.826 ±1% | ✅ |
| Potential energy Ep | 331.4 J | 300 J ±1% | ⚠️ +10.5% |
| Impact velocity v | 5.35 m/s | 5.0–5.5 m/s | ✅ |
| Empty losses p+p' | 3.63 J / 1.10% | <0.5% KN | ❌ NC |
| Knife radius | 7.9 mm | 7.5–8.5 mm | ✅ |
| Anvil spacing | 40.1 mm | 40 ±0.2 mm | ✅ |
| K̄V | Bv | b | 111.8 J | +3.8 J | 5 J | |Bv|≤10.8J | b≤16.2J | ✅ ✅ |
| U(KV) informative | 9.46 J (k=2.0) | ℹ️ §A.1.2 | ℹ️ |
| Final decision | ❌ NOT VALIDATED | Bearing maintenance | |
9. Conclusion of conformity
❌ Non-conformity: p+p' = 3.63 J (1.10%) > 0.5% KN (§6.4.5.3). Machine out of service until maintenance and new direct verification.
✅ After maintenance (simulation): p+p'=1.20 J (0.36%) ✅ | b=5 J ✅ | |Bv|=3.8 J ✅
Declaration: “Machine ZR-2019-0047 compliant with ISO 148-2 — K̄V=(111.8 ± 9.5) J (k=2.0, νKV=53) — informative §A.1.2”
Declaration: “Machine ZR-2019-0047 compliant with ISO 148-2 — K̄V=(111.8 ± 9.5) J (k=2.0, νKV=53) — informative §A.1.2”
10. Validation in real conditions — 3 CRM levels
In accordance with ISO 148-2 §7.2: minimum 2 levels, ≥5 specimens each. k determined via table E.5.
| CRM Level | K̄V (J) | b (J) | |Bv| (J) | νKV | k | U(KV) ℹ️ |
|---|---|---|---|---|---|---|
| Low (19.3 J) | 20.20 | 1 J ✅ | 0.9 J ✅ | 10.4 | 2.23 | 1.73 J |
| Medium (108 J) | 111.80 | 5 J ✅ | 3.8 J ✅ | 53 | 2.01 | 9.46 J |
| High (200 J) | 180.20 | 7.5 J ✅ | 19.8 J ✅ | 4.3 | 2.78 | 56.67 J ⚠️ |
⚠️ Normative references: ISO 148-1:2016 (Annex E) — ISO 148-2:2008/2016 (§6, §7, §8, §9, Annexes A and B) — ASTM E23 — ASTM A148 — JCGM 100:2008 (GUM) — ISO/IEC 17025:2017 — ILAC-G8:09/2019 — EA-4/02 M:2022
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